The effects of CuO loading, reaction temperature. and surface gas velocity (U-g) On the photocatalytic reduction of NO have been determined in an annular flow type and a modified two-dimensional fluidized bed photoreactor. The optimum CuO loading was found to be 3.3 wt.% and NO degradation conversion in the modified two-dimensional fluidized bed photoreactor is more than 70% at 2.5 U-mf.