A chiral aluminum solvating agent (CASA) for H-1 NMR chiral analysis of alcohols at low temperature

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A chiral aluminum solvating agent (CASA) was demonstrated to be a general and efficient reagent for H-1 NMR chiral analysis of alcohols. The sodium salt of the CASA (CASA-Na) showed a complete baseline peak separation of the hydroxyl group for various chiral alcohols including primary, secondary, and tertiary alcohols with alkyl and aryl substituents in CD3CN. Due to the weak intermolecular interaction, H-1 NMR measurement at low temperature (-40 to 10 degrees C) was required.
Publisher
ROYAL SOC CHEMISTRY
Issue Date
2018-06
Language
English
Article Type
Article
Citation

CHEMICAL COMMUNICATIONS, v.54, no.50, pp.6804 - 6807

ISSN
1359-7345
DOI
10.1039/c8cc00574e
URI
http://hdl.handle.net/10203/244569
Appears in Collection
CH-Journal Papers(저널논문)
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