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College of Natural Sciences(자연과학대학)Dept. of Chemistry(화학과)CH-Journal Papers(저널논문)

A chiral aluminum solvating agent (CASA) for H-1 NMR chiral analysis of alcohols at low temperature

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dc.contributor.authorSeo, Min Seobko
dc.contributor.authorJang, Suminko
dc.contributor.authorKim, Hyunwooko
dc.date.accessioned2018-07-24T02:59:32Z-
dc.date.available2018-07-24T02:59:32Z-
dc.date.created2018-07-16-
dc.date.created2018-07-16-
dc.date.created2018-07-16-
dc.date.created2018-07-16-
dc.date.issued2018-06-
dc.identifier.citationCHEMICAL COMMUNICATIONS, v.54, no.50, pp.6804 - 6807-
dc.identifier.issn1359-7345-
dc.identifier.urihttp://hdl.handle.net/10203/244569-
dc.description.abstractA chiral aluminum solvating agent (CASA) was demonstrated to be a general and efficient reagent for H-1 NMR chiral analysis of alcohols. The sodium salt of the CASA (CASA-Na) showed a complete baseline peak separation of the hydroxyl group for various chiral alcohols including primary, secondary, and tertiary alcohols with alkyl and aryl substituents in CD3CN. Due to the weak intermolecular interaction, H-1 NMR measurement at low temperature (-40 to 10 degrees C) was required.-
dc.languageEnglish-
dc.publisherROYAL SOC CHEMISTRY-
dc.titleA chiral aluminum solvating agent (CASA) for H-1 NMR chiral analysis of alcohols at low temperature-
dc.typeArticle-
dc.identifier.wosid000436029000031-
dc.identifier.scopusid2-s2.0-85048819732-
dc.type.rimsART-
dc.citation.volume54-
dc.citation.issue50-
dc.citation.beginningpage6804-
dc.citation.endingpage6807-
dc.citation.publicationnameCHEMICAL COMMUNICATIONS-
dc.identifier.doi10.1039/c8cc00574e-
dc.contributor.localauthorKim, Hyunwoo-
dc.description.isOpenAccessN-
dc.type.journalArticleArticle-
dc.subject.keywordPlusNMR-SPECTROSCOPY-
dc.subject.keywordPlusABSOLUTE-CONFIGURATION-
dc.subject.keywordPlusENANTIOMERIC EXCESS-
dc.subject.keywordPlusCARBOXYLIC-ACIDS-
dc.subject.keywordPlusALPHA-HYDROXY-
dc.subject.keywordPlusDISCRIMINATION-
dc.subject.keywordPlusASSIGNMENT-
dc.subject.keywordPlusCYCLODEXTRINS-
dc.subject.keywordPlusCOMPLEXES-
dc.subject.keywordPlusREAGENT-
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CH-Journal Papers(저널논문)
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