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College of Engineering(공과대학)Dept. of Nuclear and Quantum Engineering(원자력및양자공학과)NE-Journal Papers(저널논문)

Radical-mediated synthesis of trifluoroethyl amines and trifluoromethyl ketones from alkyl iodides

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dc.contributor.authorKim, Sung Gakko
dc.contributor.authorKavali, Rko
dc.date.accessioned2013-03-04T19:16:59Z-
dc.date.available2013-03-04T19:16:59Z-
dc.date.created2012-02-06-
dc.date.created2012-02-06-
dc.date.issued2002-09-
dc.identifier.citationTETRAHEDRON LETTERS, v.43, no.40, pp.7189 - 7191-
dc.identifier.issn0040-4039-
dc.identifier.urihttp://hdl.handle.net/10203/83790-
dc.description.abstractRadical reaction of alkyl iodides with trifluoromethyl phenylsulfonyl oxime ether 10 and hexamethylditin at 300 nm in benzene afforded the corresponding trifluoromethyl oxime ethers 11 in high yields, which were reduced into the 2,2,2-trifluoroethyl amines with lithium aluminium hydride. The trifluoroethyl amines could be converted into the corresponding trifluoromethyl ketones by treatment with NBS and DBU. (C) 2002 Elsevier Science Ltd. All rights reserved.-
dc.languageEnglish-
dc.publisherPERGAMON-ELSEVIER SCIENCE LTD-
dc.subjectOXIME ETHERS-
dc.subjectACYLATION APPROACH-
dc.subjectCARBOXYLIC-ACIDS-
dc.subjectESTERS-
dc.subject(TRIFLUOROMETHYL)TRIMETHYLSILANE-
dc.subjectREAGENTS-
dc.subjectINHIBITORS-
dc.subjectREDUCTION-
dc.titleRadical-mediated synthesis of trifluoroethyl amines and trifluoromethyl ketones from alkyl iodides-
dc.typeArticle-
dc.identifier.wosid000178047100015-
dc.identifier.scopusid2-s2.0-0037201089-
dc.type.rimsART-
dc.citation.volume43-
dc.citation.issue40-
dc.citation.beginningpage7189-
dc.citation.endingpage7191-
dc.citation.publicationnameTETRAHEDRON LETTERS-
dc.contributor.localauthorKim, Sung Gak-
dc.contributor.nonIdAuthorKavali, R-
dc.type.journalArticleArticle-
dc.subject.keywordAuthorradicals and radical reactions-
dc.subject.keywordAuthorfluorine and compounds-
dc.subject.keywordAuthoracylation-
dc.subject.keywordAuthorketones-
dc.subject.keywordAuthoramines-
dc.subject.keywordAuthorsulfones-
dc.subject.keywordAuthoroximes-
dc.subject.keywordPlusOXIME ETHERS-
dc.subject.keywordPlusACYLATION APPROACH-
dc.subject.keywordPlusCARBOXYLIC-ACIDS-
dc.subject.keywordPlusESTERS-
dc.subject.keywordPlus(TRIFLUOROMETHYL)TRIMETHYLSILANE-
dc.subject.keywordPlusREAGENTS-
dc.subject.keywordPlusINHIBITORS-
dc.subject.keywordPlusREDUCTION-
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