Ni-Catalyzed Intermolecular C(sp3)-H Amidation Tuned by Bidentate Directing Groups

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We disclose herein a directing group-assisted nickel-catalyzed intermolecular C(sp3)-H amidation using organic azides as nitrene precursors. With the installation of an electronically tailored directing group, enhanced amidation efficiency was achieved. A series of experimental and computational studies suggested that a putative nickel(III)-nitrenoid species is a key intermediate in the C-N bond-forming process.
Publisher
AMER CHEMICAL SOC
Issue Date
2021-02
Language
English
Article Type
Article
Citation

ACS CATALYSIS, v.11, no.5, pp.3067 - 3072

ISSN
2155-5435
DOI
10.1021/acscatal.1c00070
URI
http://hdl.handle.net/10203/291131
Appears in Collection
CH-Journal Papers(저널논문)
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