Formation of silica/poly(p-dioxanone) microspheres by surface-initiated polymerization

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A polymeric film of a biodegradable poly(p-dioxanone) was grown from 490 nm silica particles by monolayer formation via self-assembly of hydroxy-terminated triethoxysilane and subsequent surface initiated ring-opening polymerization of p-dioxanone. The resulting silica/poly(p-dioxanone) hybrid particles were characterized by means of H-1 NMR spectroscopy, IR spectroscopy, thermogravimetric analysis, field emission scanning electron microscopy, and energy-dispersive X-ray spectroscopy.
Publisher
WILEY-V C H VERLAG GMBH
Issue Date
2003-02
Language
English
Article Type
Article
Keywords

TRANSFER RADICAL POLYMERIZATION; SELF-ASSEMBLED MONOLAYERS; OPENING METATHESIS POLYMERIZATION; LIVING CATIONIC POLYMERIZATION; N-ISOPROPYLACRYLAMIDE; SILICON SURFACES; AQUEOUS-MEDIA; BRUSHES; GROWTH; GOLD

Citation

MACROMOLECULAR RAPID COMMUNICATIONS, v.24, no.2, pp.207 - 210

ISSN
1022-1336
URI
http://hdl.handle.net/10203/13063
Appears in Collection
CH-Journal Papers(저널논문)
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