FAST AND EFFICIENT SYNTHESIS OF SULFINAMIDES BY THE OXIDATION OF SULFENAMIDES USING POTASSIUM FLUORIDE AND m-CHLOROPEROXYBENZOIC ACID

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A procedure for the synthesis of N-alkyl-, N-cycloalkyl-, N,N-dialkyl-, and N-arylarenesulfinamides from the corresponding sulfenamides using KF/m-chloroperoxybenzoic acid (CPBA) in CH3CN-H2O is described. High efficiency (fast reactions, ease of manipulation, and good yields) and absence of overoxidation are the major advantageous features of this protocol.
Publisher
TAYLOR & FRANCIS INC
Issue Date
2012
Language
English
Article Type
Article
Keywords

THIOOXIME S-OXIDES; SULFUR-NITROGEN BOND; ASYMMETRIC-SYNTHESIS; KF/M-CPBA; SULFOXIDES; CHEMISTRY; SULFONAMIDES; DERIVATIVES; DISULFIDES; KETONES

Citation

SYNTHETIC COMMUNICATIONS, v.42, no.12, pp.1760 - 1769

ISSN
0039-7911
DOI
10.1080/00397911.2010.543748
URI
http://hdl.handle.net/10203/101589
Appears in Collection
CH-Journal Papers(저널논문)
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