Condensation reaction of 3-(methacryloxypropyl)-trimethoxysilane and diisobutylsilanediol in non-hydrolytic sol-gel process

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The condensation reaction of 3-methacryloxypropyl-trimethoxysilane (MPTS) and diisobutylsilanediol (DIBSD) in a non-hydrolytic sol-gel process was investigated in terms of the reaction time and the catalyst amount for fabrication of inorganic-organic hybrid materials. The degree of condensation, which was characterized by Si-29 NMR, H-1 NMR and Abbe refractometry, increases with increased the reaction time and greater catalyst amount. However, a the large catalyst amount breaks the methacryl group during the condensation reaction. Thus, the reaction time and the catalyst amount were optimized to synthesize the condensed methacryl oligosiloxanes.
Publisher
SPRINGER
Issue Date
2006-09
Language
English
Article Type
Article
Keywords

HYBRID MATERIALS

Citation

JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, v.39, no.3, pp.255 - 260

ISSN
0928-0707
DOI
10.1007/s10971-006-7884-y
URI
http://hdl.handle.net/10203/9698
Appears in Collection
MS-Journal Papers(저널논문)
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