A facile synthetic route to (+)-allosedamine via hydrolytic kinetic resolution and olefin metathesis

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A concise synthesis of (+)-allosedamine has been achieved using cobalt-catalyzed hydrolytic kinetic resolution (HKR) and ruthenium-catalyzed ring closing metathesis (RCM) as two key steps, in which HKR was used to introduce both stereogenic centers in the natural compound with a high degree of diastereomeric ratio and cyclization was carried out with the well developed RCM procedure. (C) 2004 Elsevier Ltd. All rights reserved.
Publisher
PERGAMON-ELSEVIER SCIENCE LTD
Issue Date
2004-08
Language
English
Article Type
Article
Keywords

RING-CLOSING METATHESIS; RUTHENIUM BY-PRODUCTS; ASYMMETRIC-SYNTHESIS; CROSS-METATHESIS; PIPERIDINE ALKALOIDS; MITSUNOBU REACTION; TERMINAL EPOXIDES; OPENING REACTIONS; CONVENIENT METHOD; TANDEM CATALYSIS

Citation

TETRAHEDRON, v.60, no.34, pp.7353 - 7359

ISSN
0040-4020
URI
http://hdl.handle.net/10203/82183
Appears in Collection
CH-Journal Papers(저널논문)
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