Nickel/Briphos-Catalyzed Direct Transamidation of Unactivated Secondary Amides Using Trimethylsilyl Chloride

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Direct transamidation of secondary amides was developed via nickel catalysis. In the presence of trimethylsilyl chloride and manganese, Ni(diglyme)Cl-2 with a Briphos ligand efficiently promoted the transamidation of N-aryl benzamide derivatives with primary amines to afford the corresponding secondary amides in moderate to good yields. Primary amines bearing electron-donating groups gave higher yields of the transamidation products.
Publisher
AMER CHEMICAL SOC
Issue Date
2018-12
Language
English
Article Type
Article
Citation

ORGANIC LETTERS, v.20, no.23, pp.7563 - 7566

ISSN
1523-7060
DOI
10.1021/acs.orglett.8b03304
URI
http://hdl.handle.net/10203/249007
Appears in Collection
CH-Journal Papers(저널논문)
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