Quantitative determination of uranium and europium in glass matrix by laser-induced breakdown spectroscopy

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Laser-induced breakdown spectroscopy was applied to the quantitative determination of the elemental composition of glass samples containing U and Eu as a surrogate for highly radioactive glass waste. The emission intensities of both major and minor elements in the samples were measured simultaneously in the wavelength range from 200 to 780 nm by using an echelle spectrometer. Calibration curves for the concentration determination were obtained from the emission intensities at 358.488 nm for U 1, and 459.403 nm for Eu 1. Limits of detection for U and Eu were similar to 150 and similar to 4.2 parts per million, respectively. (C) 2011 Elsevier B.V. All rights reserved.
Publisher
PERGAMON-ELSEVIER SCIENCE LTD
Issue Date
2011
Language
English
Article Type
Article
Keywords

ONLINE MULTIELEMENT ANALYSIS; EMISSION-SPECTROSCOPY; SPECTROMETRY; PLASMA; ABLATION; SAMPLES; PULSE; MELT

Citation

SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, v.66, no.9-10, pp.761 - 764

ISSN
0584-8547
DOI
10.1016/j.sab.2011.09.002
URI
http://hdl.handle.net/10203/103898
Appears in Collection
NE-Journal Papers(저널논문)
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