FAST AND EFFICIENT SYNTHESIS OF SULFINAMIDES BY THE OXIDATION OF SULFENAMIDES USING POTASSIUM FLUORIDE AND m-CHLOROPEROXYBENZOIC ACID
A procedure for the synthesis of N-alkyl-, N-cycloalkyl-, N,N-dialkyl-, and N-arylarenesulfinamides from the corresponding sulfenamides using KF/m-chloroperoxybenzoic acid (CPBA) in CH3CN-H2O is described. High efficiency (fast reactions, ease of manipulation, and good yields) and absence of overoxidation are the major advantageous features of this protocol.
- Publisher
- TAYLOR & FRANCIS INC
- Issue Date
- 2012
- Language
- English
- Article Type
- Article
- Keywords
THIOOXIME S-OXIDES; SULFUR-NITROGEN BOND; ASYMMETRIC-SYNTHESIS; KF/M-CPBA; SULFOXIDES; CHEMISTRY; SULFONAMIDES; DERIVATIVES; DISULFIDES; KETONES
- Citation
SYNTHETIC COMMUNICATIONS, v.42, no.12, pp.1760 - 1769
- ISSN
- 0039-7911
- Appears in Collection
- CH-Journal Papers(저널논문)
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